Triethylamine → HCID 69669790、化合物

HRID 241603ノート

反応式

HRID 241603 の反応式
[N:1]1([CH2:6][C:7]([O:9][CH2:10]C)=[O:8])[CH:5]=[CH:4][N:3]=[N:2]1.[CH2:12](N(CC)CC)C>CO>[N:1]1([C:6](=[CH2:12])[C:7]([O:9][CH3:10])=[O:8])[CH:5]=[CH:4][N:3]=[N:2]1

参加物

4

反応物 2

HCID 8471TriethylamineHCID 10103365Ethyl 2-(1H-1,2,3-triazol-1-YL)acetate

生成物 1

HCID 69669790HCID 69669790、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

反応条件

温度
22 °C

実験手順

450 g of ethyl 2-(1H-1,2,3-triazol-1-yl)acetate were dissolved in 3.5 1 of methanol, 30 g of triethylamine were added and the mixture was stirred at 22° C. for 16 h. All solvents were then distilled off under reduced pressure. This gave 410 g of the title compound as an oil.

後処理

  1. additionwere added
  2. distillationAll solvents were then distilled off under reduced pressure

出典と根拠

ORDレコード
ord-a65d5812e32c46648999775e580451ae
出典データセット
uspto-grants-2014_02
特許番号
US08653074B2

反応ノート

読み込み中…