化工社化工社 化学情報印刷レポート · 研究参考用
1-Butanol → Phenyltripropoxysilane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Butanol | HCID 263 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Water | HCID 962 | — |
| 反応物 | Isopropanol | HCID 3776 | — |
| 反応物 | Tetraethoxysilane | HCID 6517 | — |
| 反応物 | Phenyltriethoxysilane | HCID 13075 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | Phenyltripropoxysilane | HCID 15909578 | — |
反応手順
In a 1-liter flask 297 grams (4.798 moles) 2-propanol, 148 grams (2.558 moles) acetone, 73 grams (0.351 moles) TEOS, 45 grams (0.251 moles) MTEOS 121 grams (0.503 moles) phenyltriethoxysilane, 0.6 grams 0.1 M nitric acid and 72 grams (3.716 moles) deionized water were combined. The flask was refluxed for 4 hours. To the solution, 57 grams (0.769 moles) of Butanol, 88 grams (1.422 moles) 2-propanol, 44 grams 0.758 moles) of acetone, 59 grams (1.227 moles) of ethanol, 9.5 grams (0.528 moles) deionized water were added.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06824879B2 |
| 出典データセット | uspto-grants-2004_11 |
| ORD ID | ord-6a0aa049500446cfb73a8fc2f8f293a3 |
| 出典メモ | uspto-grants-2004_11 |