反応式
[O:1]1[C:3]2([CH2:8][CH2:7][O:6][CH2:5][CH2:4]2)[CH2:2]1.[NH4+:9].[OH-]>CO>[NH2:9][CH2:2][C:3]1([OH:1])[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1参加物
4
実験手順
The methanol solution of 1,6-dioxaspiro[2.5]octane (3.15 g, 27.6 mmol) was added to the 25% ammonia aqueous solution (50.0 mL, 27.6 mmol) at 0° C. The mixture was warmed to room temperature and stirred for 18 h. The reaction mixture was concentrated in vacuo. The crude product was used for next step reaction without purification.
後処理
- concentrationThe reaction mixture was concentrated in vacuo
- customThe crude product was used for next step reaction without purification
出典と根拠
- ORDレコード
- ord-fc00036b66ec41eeb5e44cf2df03e5b5
- 出典データセット
- uspto-grants-2014_02
- 特許番号
- US08653063B2
関連ノート
読み込み中…