化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Hydroxylauric Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 2-chlorododecanoic Acid | HCID 4387370 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Hydroxylauric Acid | HCID 97783 | — |
反応手順
0.1 Mole of alpha-chlorolauric acid prepared in the foregoing manner was admixed with 500 mls. water and 0.4 moles of KOH in a suitable reaction vessel and stirred overnight at a temperature of 98°-100° C. The reaction mixture was poured into a separatory funnel, to which was added hydrochloric acid (40 ml. conc. HCl in 200 ml. H2O). The mixture was extracted with chloroform. The chloroform layer was removed and the CHCl3 evaporated to yield alpha-hydroxylauric acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04469635 |
| 出典データセット | uspto-grants-1984_09 |
| ORD ID | ord-39e27f2d4b784cdc8dd8f06831abdd2a |
| 出典メモ | uspto-grants-1984_09 |