反応式
[Cl:1]Cl.[N+]([C:6]1[CH:11]=[CH:10][C:9]([O:12][C:13]([F:16])([F:15])[F:14])=[CH:8][CH:7]=1)([O-])=O>>[Cl:1][C:6]1[CH:11]=[CH:10][C:9]([O:12][C:13]([F:16])([F:15])[F:14])=[CH:8][CH:7]=1参加物
3
実験手順
Chlorine and p-nitrotrifluoromethoxybenzene (10.7 parts) were fed simultaneously at a molar ratio of 3:1, Cl2 :organic reactant, into a vapor phase reactor maintained at 300° C. to 320° C. over a 30 minute period to yield 8.2 parts of p-chlorotrifluoromethoxybenzene (83% yield). The structure of the product was confirmed by gas chromatographic--mass spectrum and F19 nuclear magnetic resonance analysis.
後処理
- temperatureorganic reactant, into a vapor phase reactor maintained at 300° C. to 320° C. over a 30 minute period
出典と根拠
- ORDレコード
- ord-665b3233577e40e2b738511d049dd05c
- 出典データセット
- uspto-grants-1984_09
- 特許番号
- US04470930
関連ノート
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