Methylamine → HCID 178482527、化合物
反応式
CO[C:3]1[C:7](OC)=[N:6][S:5](=[O:11])(=[O:10])[N:4]=1.[CH3:12][C:13]1[C:14]([CH2:18][S:19][CH2:20][CH2:21][NH2:22])=[N:15][O:16][N:17]=1.[CH3:23][NH2:24]>>[CH3:12][C:13]1[C:14]([CH2:18][S:19][CH2:20][CH2:21][NH:22][C:3]2[C:7]([NH:24][CH3:23])=[N:6][S:5](=[O:11])(=[O:10])[N:4]=2)=[N:15][O:16][N:17]=1参加物
4
実験手順
When a methanolic suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1,1-dioxide is successively treated with an equimolar amount of 2-[(4-methyl-1,2,5-oxadiazol-3-yl)methylthio]ethylamine [prepared in Step B] and excess methylamine by the general procedure of Example 2, the title compound is thereby produced.
出典と根拠
- ORDレコード
- ord-ac5f742e85204dc5b8a62d8cbae1b03b
- 出典データセット
- uspto-grants-1984_09
- 特許番号
- US04471122
反応ノート
読み込み中…