Water → N-(2,4-Dimethylthiophen-3-yl)-2-methoxyacetamide
反応式
[CH3:1][C:2]1[S:3][CH:4]=[C:5]([CH3:8])[C:6]=1[NH2:7].C([O-])([O-])=O.[K+].[K+].O.[CH3:16][O:17][CH2:18][C:19](Cl)=[O:20]>C(Cl)Cl>[CH3:1][C:2]1[S:3][CH:4]=[C:5]([CH3:8])[C:6]=1[NH:7][C:19](=[O:20])[CH2:18][O:17][CH3:16]参加物
6
実験手順
To 12.7 g (0.1 mol) of 2,4-dimethyl-3-aminothiophene, 13.84 g (0.1 mol) of K2CO3, 50 ml of water and 160 ml of methylene chloride are added without cooling 10.8 g (0.1 mol) of methoxyacetyl chloride.
出典と根拠
- ORDレコード
- ord-043384c35a7241f89787a6dc3bc4aabb
- 出典データセット
- uspto-grants-1984_09
- 特許番号
- US04472425
反応ノート
読み込み中…