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Hydrochloric Acid → 2-Amino-2'-[alpha-(hydroxyimino)benzyl]-4'-nitro-acetanilide hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 2-Amino-2'-[alpha-(hydroxyimino)benzyl]-4'-nitro-acetanilide | HCID 86739645 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 2-Amino-2'-[alpha-(hydroxyimino)benzyl]-4'-nitro-acetanilide hydrochloride | HCID 86739648 | — |
反応手順
Hydrogen chloride is conducted for 10 minutes into a solution of 2.7 g (8.59 mmol) of 2-amino-2'-[α-(hydroxyimino)benzyl]-4'-nitro-acetanilide in 150 ml of methylene chloride and 30 ml of ethanol. The solution is subsequently evaporated to dryness and the residue is dried at 60° overnight in vacuo. There is obtained 2-amino-2'-[α-(hydroxyimino)benzyl]-4'-nitro-acetanilide hydrochloride of melting point 150° (decomposition).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04472435 |
| 出典データセット | uspto-grants-1984_09 |
| ORD ID | ord-a0ddf31a356b41f3b2102d59c0ce943d |
| 出典メモ | uspto-grants-1984_09 |