Water → HCID 178460683、化合物
反応式
[Br:1][C:2]1[CH:8]=[C:7]([Br:9])[CH:6]=[C:5]([Br:10])[C:3]=1[NH2:4].Cl[C:12]([CH:14]([CH3:20])[CH2:15][P:16](Cl)(C)=[O:17])=[O:13].[OH2:21]>>[Br:1][C:2]1[CH:8]=[C:7]([Br:9])[CH:6]=[C:5]([Br:10])[C:3]=1[NH:4][C:12]([CH:14]([CH3:20])[CH2:15][PH:16](=[O:21])[OH:17])=[O:13]参加物
4
実験手順
330 g (1 mol) of 2,4,6-tribromoaniline was reacted as described in Example 1 with 207 g (1.02 mol) of [2-(chloroformyl-)2-(methyl)ethyl-]methyl phosphinic acid chloride (prepared as described by V. K. Khairullin et al., C.A. 69, 106816 k (1968)). After hydrolysis with 6 liters of water, the resulting [2-(2,4,6-tribromophenylcarbamoyl-) 2-(methyl)ethyl-]methyl phosphinic acid was filtered off and dried at 80° C under vacuum.
後処理
- filtrationthe resulting [2-(2,4,6-tribromophenylcarbamoyl-) 2-(methyl)ethyl-]methyl phosphinic acid was filtered off
- customdried at 80° C under vacuum
出典と根拠
- ORDレコード
- ord-fec1a8bdd3a7421f978ddd31854bd6cd
- 出典データセット
- uspto-grants-1978_08
- 特許番号
- US04105689
反応ノート
読み込み中…