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4-Diisopropylamino-2-phenyl-butyronitrile → alpha,alpha-Bis[2-(diisopropylamino)ethyl]-alpha-(2-pyridyl)acetonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Diisopropylamino-2-phenyl-butyronitrile | HCID 12612210 | — |
| 反応物 | 4-Diisopropylamino 2-(2-pyridyl)butyronitrile | HCID 13319674 | — |
| 生成物 | alpha,alpha-Bis[2-(diisopropylamino)ethyl]-alpha-(2-pyridyl)acetonitrile | HCID 21320525 | — |
反応手順
Substitution of an equivalent quantity of the preceding acetonitrile for α-[2-(diisopropylamino)ethyl]-α-phenylacetonitrile called for in Example 2, Method B and substantial repetition of the procedure detailed in that example, affords α,α-bis[2-(diisopropylamino)ethyl]-α-(2-pyridyl)acetonitrile, as an oil boiling at about 155°-160° C. at 0.3 mm. pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04107205 |
| 出典データセット | uspto-grants-1978_08 |
| ORD ID | ord-9deea0d92c104e0da26a9d4ff47f464d |
| 出典メモ | uspto-grants-1978_08 |