Phosphorus pentachloride → HCID 20314298、化合物

HRID 2419819ノート

反応式

[F:1][C:2]([F:16])([F:15])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10](=O)[CH2:11][CH2:12][CH3:13].P(Cl)(Cl)(Cl)(Cl)[Cl:18]>>[F:1][C:2]([F:16])([F:15])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]=[C:10]([Cl:18])[CH2:11][CH2:12][CH3:13]

参加物

反応物 2

HCID 24819Phosphorus pentachloride

HCID 3557464N-[2-(Trifluoromethyl)phenyl]butanamide

生成物 1

HCID 20314298HCID 20314298、化合物収率 99.4%

実験手順

Using the procedure of Step B of Example 6, 23.1 g of the product of Step A and 22.9 g of phosphorus pentachloride were reacted to form 24.8 g of N-(2-trifluoromethylphenyl)-butanimidoyl chloride as an oil which was used as is for the next step.

後処理

customwere reacted

出典と根拠

ORDレコード: ord-9de2ae9aa1044ce3b926273357e49a05
出典データセット: uspto-grants-1978_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04107310

反応ノート

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