Azolimine → HCID 178482452、化合物

HRID 2420359ノート

反応式

HRID 2420359 の反応式
[C:1]1([N:7]2[CH2:11][C:10](=[O:12])[N:9](C)[C:8]2=[NH:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:15][O-].[Na+]>>[C:1]1([N:7]2[CH2:11][C:10](=[O:12])[N:9]=[C:8]2[NH:14][CH3:15])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

参加物

3

反応物 2

HCID 38684AzolimineHCID 10942334Sodium Methoxide

生成物 1

HCID 178482452HCID 178482452、化合物

実験手順

2.2 g. of 1-phenyl-2-imino-3-methyl-4-oxoimidazolidine, 0.26 g. of sodium methoxide and 65 ml. of absolute alcohol were heated to reflux for 20 hours. The insoluble solid was filtered and ethanol was evaporated leaving a yellow solid.

後処理

  1. temperatureto reflux for 20 hours
  2. filtrationThe insoluble solid was filtered
  3. customethanol was evaporated
  4. customleaving a yellow solid

出典と根拠

ORDレコード
ord-9b44321f0dda43b69bcb7a3239f97f60
出典データセット
uspto-grants-1978_08
特許番号
US04110445

反応ノート

読み込み中…