3,4-Dichloroaniline → HCID 19006421、化合物
反応式
[Cl:1][C:2]1[CH:14]=[CH:13][CH:12]=[C:11]([Cl:15])[C:3]=1[C:4]([NH:6][C:7](=[S:10])[SH-]C)=[S:5].[Cl:16][C:17]1[CH:18]=[C:19]([CH:21]=[CH:22][C:23]=1[Cl:24])[NH2:20]>C1(C)C=CC=CC=1>[Cl:15][C:11]1[CH:12]=[CH:13][CH:14]=[C:2]([Cl:1])[C:3]=1[C:4]([NH:6][C:7]([NH:20][C:19]1[CH:21]=[CH:22][C:23]([Cl:24])=[C:17]([Cl:16])[CH:18]=1)=[S:10])=[S:5]参加物
4
実験手順
3.0 g of N-(2,6-dichlorothiobenzoyl)-S-methyl-dithiocarbamate and 1.6 g of 3,4-dichloroaniline are dissolved in 25 ml of toluene and subsequently heated while refluxing for 5 hours. The resulting yellow precipitate is worked up in the usual manner. Yield 2.1 g. Melting point 168°-170° C.
後処理
- temperaturesubsequently heated
- temperaturewhile refluxing for 5 hours
出典と根拠
- ORDレコード
- ord-171055c28d3240a4a4a6921c59c5d922
- 出典データセット
- uspto-grants-1978_08
- 特許番号
- US04110469
反応ノート
読み込み中…