化工社化工社 化学情報印刷レポート · 研究参考用
Carbon Dioxide → Zinc sorbate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carbon Dioxide | HCID 280 | — |
| 反応物 | Zinc Carbonate | HCID 19005 | — |
| 反応物 | Sorbic Acid | HCID 643460 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Zinc sorbate | HCID 6437346 | — |
反応手順
224 g sorbic acid were added to 1,000 ml ethanol. While stirring, 117 g basic zinc carbonate was added incrementally at room temperature. The mixture formed a readily stirrable suspension. At room temperature, stirring was continued and, after a short delay, the formation of CO2 started which showed that the reaction was occurring. After 24 hours, enough zinc sorbate had formed so that a firm mass had formed. In a rotary evaporator, the ethanol was drawn off at 60° under vacuum. A white mass of zinc disorbate was recovered and ground in a mill.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07959530B2 |
| 出典データセット | uspto-grants-2011_06 |
| ORD ID | ord-ee60136b9bb64f2784b7827353b8b5c6 |
| 出典メモ | uspto-grants-2011_06 |