3,5-Dichloroaniline → N-(Benzimidazol-2-yl)-3,5-dichloroaniline

HRID 2423042ノート

反応式

HRID 2423042 の反応式
Cl[C:2]1[NH:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[Cl:11][C:12]1[CH:13]=[C:14]([CH:16]=[C:17]([Cl:19])[CH:18]=1)[NH2:15]>>[N:6]1[C:5]2[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=2[NH:3][C:2]=1[NH:15][C:14]1[CH:13]=[C:12]([Cl:11])[CH:18]=[C:17]([Cl:19])[CH:16]=1

参加物

3

反応物 2

HCID 122813,5-DichloroanilineHCID 785722-Chlorobenzimidazole

生成物 1

HCID 923869N-(Benzimidazol-2-yl)-3,5-dichloroaniline

実験手順

The title compound was prepared from 2-chlorobenzimidazole and 3,5-dichloroaniline by Procedure A. The product was isolated by filtration to give the title compound as a hydrochloride salt (solid, mp 317-318° C.). MS(ES+) m/z 278 (M+, 100).

後処理

  1. customThe product was isolated by filtration

出典と根拠

ORDレコード
ord-e7efba7cd8ab49f996b94c8b27d1185e
出典データセット
uspto-grants-2011_06
特許番号
US07960561B2

反応ノート

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