化工社化工社 化学情報印刷レポート · 研究参考用
1,3-Dibromopropane → Ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Dibromopropane | HCID 8001 | — |
| 反応物 | Ethyl 3-pyridylacetate | HCID 96490 | — |
| 生成物 | Ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate | HCID 67246748 | — |
反応手順
Prepared in a similar manner to that described above by reacting ethyl 2-pyridin-3-ylacetate with 1,3-dibromopropane to give ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate which was then hydrogenated to give the desired compound as a brown oil (quantitative reaction).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07964618B2 |
| 出典データセット | uspto-grants-2011_06 |
| ORD ID | ord-f374677e9bf0408cab463ad44f34a638 |
| 出典メモ | uspto-grants-2011_06 |