3,5-Diisopropyl-4-methoxybenzaldehyde → 3-(3,5-Diisopropyl-4-methoxybenzylidene)-4-methyl-1,3-dihydroindol-2-one

反応式

[CH:1]([C:4]1[CH:5]=[C:6]([CH:9]=[C:10]([CH:14]([CH3:16])[CH3:15])[C:11]=1[O:12][CH3:13])[CH:7]=O)([CH3:3])[CH3:2].[CH3:17][C:18]1[CH:26]=[CH:25][CH:24]=[C:23]2[C:19]=1[CH2:20][C:21](=[O:27])[NH:22]2>>[CH:1]([C:4]1[CH:5]=[C:6]([CH:9]=[C:10]([CH:14]([CH3:16])[CH3:15])[C:11]=1[O:12][CH3:13])[CH:7]=[C:20]1[C:19]2[C:23](=[CH:24][CH:25]=[CH:26][C:18]=2[CH3:17])[NH:22][C:21]1=[O:27])([CH3:3])[CH3:2]

参加物

反応物 2

HCID 105850253,5-Diisopropyl-4-methoxybenzaldehyde

HCID 125793824-Methyl-1,3-dihydro-2H-indol-2-one

生成物 1

HCID 542959033-(3,5-Diisopropyl-4-methoxybenzylidene)-4-methyl-1,3-dihydroindol-2-one

実験手順

3,5-Diisopropyl-4-methoxybenzaldehyde was condensed with 4-methyl-2-oxindole to give 0.3 g of 3-(3,5-diisopropyl-4-methoxybenzylidene)-4-methyl-1,3-dihydroindol-2-one as a yellow-orange solid.

出典と根拠

ORDレコード: ord-73e83ea33aab42c38cab96b7049f0674
出典データセット: uspto-grants-2005_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06855730B2

反応ノート

読み込み中…