化工社化工社 化学情報印刷レポート · 研究参考用
(3-Bromophenyl)acetic acid → Ethyl 3-(bromophenyl)acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3-Bromophenyl)acetic acid | HCID 74653 | — |
| 反応物 | Ethyl 2-(4-bromophenyl)acetate | HCID 7020609 | — |
| 生成物 | Ethyl 3-(bromophenyl)acetate | HCID 11470552 | — |
反応手順
Employing the same general procedure as for the preparation of ethyl (4-bromophenyl)acetate (Compound A), 100 g (463 mmol) of 3-bromophenylacetic acid was converted into the title compound (yellow oil) using 2 g of conc. H2SO4 and 500 ml of ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06855832B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-13b89fea485a4edfacf2184795d38ef0 |
| 出典メモ | uspto-grants-2005_02 |