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4,4-Dimethyl-7-bromo-1-phenylthio-3,4-dihydronaphthalene → 4,4-Dimethyl-7-acetyl-1-phenylthio-3,4-dihydronaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4,4-Dimethyl-7-bromo-1-phenylthio-3,4-dihydronaphthalene | HCID 15896018 | — |
| 反応物 | 3,4-dihydro-4,4-dimethyl-7-acetyl-1(2H)-naphthalenone | HCID 22323726 | — |
| 生成物 | 4,4-Dimethyl-7-acetyl-1-phenylthio-3,4-dihydronaphthalene | HCID 12070988 | — |
反応手順
Employing the procedure used for the preparation of 4,4-dimethyl-7-acetyl-3,4-dihydronaphthalen-1(2H)-one (Compound C1) 1.2 g, (3.5 mmol) of 4,4-dimethyl-7-Bromo-1-phenylthio-3,4-dihydronaphthalene (Compound A35) was converted to the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06855832B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-7ac6f5c6953746b4bac3956fd81beed3 |
| 出典メモ | uspto-grants-2005_02 |