Hydrochloric Acid → Methyl 2,6-dichlorophenylacetate

HRID 24671ノート

反応式

HRID 24671 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[CH2:9][C:10]([OH:12])=[O:11].Cl.[CH3:14]O>>[CH3:14][O:11][C:10](=[O:12])[CH2:9][C:3]1[C:2]([Cl:1])=[CH:7][CH:6]=[CH:5][C:4]=1[Cl:8]

参加物

4

反応物 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 810582,6-Dichlorophenylacetic acid

生成物 1

HCID 2734107Methyl 2,6-dichlorophenylacetate

実験手順

(2,6-Dichlorophenyl)acetic acid (2.55 g) was dissolved in anhydrous MeOH (60 mL) and HCl (gas) was passed through the mixture and the resulting solution was stirred at room temperature for 18 h. The solvent was then evaporated to give (2,6-dichlorophenyl)acetic acid methyl ester (2.7 g).

後処理

  1. customThe solvent was then evaporated

出典と根拠

ORDレコード
ord-90bb675ddfda4fec9b754c7947ac0371
出典データセット
uspto-grants-2005_02
特許番号
US06855843B2

反応ノート

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