化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → 6-Hydroxyindole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | 3-Amino-p-cresol | HCID 17820 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | 6-Hydroxyindole | HCID 524508 | 38% |
反応手順
The semicarbazone obtained above was reduced catalytically using 10% palladium on carbon in ethanol to yield a mixture of 6-hydroxyindole 38% yield, mp 124°-6° C., and 3-amino-4-methylphenol which were separated by column chromatography.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04704390 |
| 出典データセット | uspto-grants-1987_11 |
| ORD ID | ord-7cd80c3b6edb4a3a9f9b461fd0442c69 |
| 出典メモ | uspto-grants-1987_11 |