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HRID 246899作成日:2026年10月26日

Chlorine → Benzene, 2-chloro-1-fluoro-4-(trifluoromethyl)-

https://huagongshe.com/reaction/246899

反応式

関与物質

役割名称HCID仕込み量
反応物ChlorineHCID 24526—
反応物4-Fluoro-3-nitrobenzotrifluorideHCID 67778—
生成物Benzene, 2-chloro-1-fluoro-4-(trifluoromethyl)-HCID 157153—

反応条件

温度320 °C

反応手順

In a continuous process, about 8 parts per hour of 4-fluoro-3-nitrobenzotrifluoride vapors and about 15 parts per hour of chlorine gas were passed simultaneously through a vapor phase reactor maintained at a temperature of about 320° C. and the reaction product vapors were condensed and collected. The process was continued until about 40 parts of 4-fluoro-3-nitrobenzotrifluoride had been passed through the reactor, yielding about 36.3 parts of 3-chloro-4-fluorobenzotrifluoride product. The structure of the product was confirmed by spectral analysis.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04704483
出典データセットuspto-grants-1987_11
ORD IDord-6e8d9d79d995455cab8dcd5b56d5a2fd
出典メモuspto-grants-1987_11