関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Chlorine | HCID 24526 | — |
| 反応物 | 4-Fluoro-3-nitrobenzotrifluoride | HCID 67778 | — |
| 生成物 | Benzene, 2-chloro-1-fluoro-4-(trifluoromethyl)- | HCID 157153 | — |
反応手順
In a continuous process, about 8 parts per hour of 4-fluoro-3-nitrobenzotrifluoride vapors and about 15 parts per hour of chlorine gas were passed simultaneously through a vapor phase reactor maintained at a temperature of about 320° C. and the reaction product vapors were condensed and collected. The process was continued until about 40 parts of 4-fluoro-3-nitrobenzotrifluoride had been passed through the reactor, yielding about 36.3 parts of 3-chloro-4-fluorobenzotrifluoride product. The structure of the product was confirmed by spectral analysis.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04704483 |
|---|
| 出典データセット | uspto-grants-1987_11 |
|---|
| ORD ID | ord-6e8d9d79d995455cab8dcd5b56d5a2fd |
|---|
| 出典メモ | uspto-grants-1987_11 |
|---|