Monochloramine → Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1)

HRID 247141

反応式

HRID 247141 の反応式
C[CH:2]1[O:7][CH:6](C)[CH2:5][N:4]([CH2:9][CH:10](O)C)[CH2:3]1.[Cl:13]N>>[ClH:13].[Cl:13][CH2:10][CH2:9][N:4]1[CH2:5][CH2:6][O:7][CH2:2][CH2:3]1

参加物

3

反応物 2

HCID 25423MonochloramineHCID 98999alpha,2,6-Trimethylmorpholin-4-ylethanol

生成物 1

HCID 77210Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1)

実験手順

An amount, 398.5 grams, of 2,6-dimethyl-N-(2-hydroxypropyl) morpholine (2.3 moles) was condensed with the free chloroamine obtained from 390.5 grams N-chloroethyl morpholine hydrochloride (2.3 moles) as described above to give 325.4 grams (55.7%) of the catalyst as a pale yellow oil, bp 122°-124° C. at 0.3 mm of Hg. The structure was confirmed by elemental analysis, calc. 62.9 C, 10.6 H, 9.8 N; found 62.2 C, 10.4 H, 9.8 N.

出典と根拠

ORDレコード
ord-400f9a2158ad4561af5265f73f0641f7
出典データセット
uspto-grants-1987_11
特許番号
US04705840

関連ノート

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