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Monochloramine → 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Monochloramine | HCID 25423 | — |
| 反応物 | alpha,2,6-Trimethylmorpholin-4-ylethanol | HCID 98999 | — |
| 生成物 | 4-(2-Chloro-ethyl)-2,6-dimethyl-morpholine hydrochloride | HCID 12955539 | — |
反応手順
An amount, 389.3 grams, of 2,6-dimethyl-N-(2-hydroxypropyl) morpholine (2.25 moles) was condensed with the free chloroamine obtained from 481.5 grams N-chloroethyl-2,6-dimethylmorpholine hydrochloride (2.25 moles) as described above to give 415.9 grams (58.8%) of the catalyst, bp 127°-129° C. at 0.3 mm of Hg. The structure was confirmed as that of the title compound by elemental analysis, calc. 64.9 C, 10.9 H, 8.9 N; found 64.4 C, 10.6 H, 8.9 N.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04705840 |
| 出典データセット | uspto-grants-1987_11 |
| ORD ID | ord-2bf37e33554e4fd9b07d5dfa61613237 |
| 出典メモ | uspto-grants-1987_11 |