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Ethyl 3-aminobenzoate → 3-[[(Z)-(2-oxo-1H-indol-3-ylidene)-phenylmethyl]amino]benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl 3-aminobenzoate | HCID 11400 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1-Benzoyl-3-(1-chloro-1-phenyl-methylidene)-2-indolinone | HCID 54432648 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 3-[[(Z)-(2-oxo-1H-indol-3-ylidene)-phenylmethyl]amino]benzoic acid | HCID 178517081 | — |
反応手順
Prepared analogously to Example 2c from 1-benzoyl-3-(1-chloro-1-phenyl-methylidene)-2-indolinone and ethyl 3-aminobenzoate and subsequent total saponification with sodium hydroxide solution in methanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06855710B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-8601aa90fc2d48c88bd3f1cf1d90f95b |
| 出典メモ | uspto-grants-2005_02 |