関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | Lauryl Methacrylate | HCID 8906 | — |
| 反応物 | 2,2'-Azobis(2,4-dimethylvaleronitrile) | HCID 91537 | — |
| 生成物 | Laurylmethacrylate Acrylic Acid | HCID 86741893 | 33% |
反応手順
To 795.4 g of laurylmethacrylate is added 4.64 g of glacial acrylic acid and 800 g of liquid hydrocarbon sold commercially as Isopar® M by Exxon. Then 0.8 g of 2,2'-azobis(2,4-dimethylvaleronitrile) which is sold commercially as Vazo® 52 by E. I. duPont de Nemours Corporation is added. The solution is agitated, purged with nitrogen for 1 hour and then heated to 50° C. After 12 hours of heating, the temperature of the thickened solution is increased to 60° C. and held there for 2 hours. It is then cooled and mixed with another 800 g of the aforementioned liquid hydrocarbon to give a 33 percent polymer solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04708997 |
|---|
| 出典データセット | uspto-grants-1987_11 |
|---|
| ORD ID | ord-3123c02ade5f478e8cb06b0adcc5a922 |
|---|
| 出典メモ | uspto-grants-1987_11 |
|---|
