関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethylene carbonate | HCID 7303 | — |
| 反応物 | 1,4-Butanediol | HCID 8064 | — |
| 触媒 | Sodium Stannate | HCID 21977542 | — |
| 生成物 | Carbon Dioxide | HCID 280 | 19.3% |
| 生成物 | Ethylene carbonate | HCID 7303 | 93% |
反応手順
A 10:1 mole ratio of ethylene carbonate to 1,4-butanediol is heated with stirring under a nitrogen atmosphere for 7 hours at 150° C. using 0.5 percent sodium stannate trihydrate as catalyst to give 93 percent ethylene carbonate conversion to a poly(alkylene carbonate) polyol with 19.3 percent carbon dioxide. The catalyst is removed as in Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04709069 |
|---|
| 出典データセット | uspto-grants-1987_11 |
|---|
| ORD ID | ord-efcb62d0582146a9bcf8ff5e7cc2171a |
|---|
| 出典メモ | uspto-grants-1987_11 |
|---|
