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Chloroethane → N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide dihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloroethane | HCID 6337 | — |
| 反応物 | N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide | HCID 9890945 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | N-Methyl-N-{[1-[3-(p-fluorophenoxy)propyl]-4-piperidyl]methyl}-5-isoquinolinesulfonamide dihydrochloride | HCID 19764599 | — |
反応手順
5.5 g of the compound obtained in stage A is taken up in 10 cm3 of acetonitrile. 7.5 cm3 of a 3.3N solution of hydrochloric ether are added to this solution. 3.1 g of a solid which corresponds to the title compound are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05208243 |
| 出典データセット | uspto-grants-1993_05 |
| ORD ID | ord-5e7f19ff56af4ccabb05d3f49423a133 |
| 出典メモ | uspto-grants-1993_05 |