化工社化工社 化学情報印刷レポート · 研究参考用
4-Methylbenzenethiol → 3-Bromo-5-trifluoromethylphenyl 4-tolyl sulphide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methylbenzenethiol | HCID 7811 | — |
| 反応物 | 3-Bromo-5-fluorobenzotrifluoride | HCID 2736323 | — |
| 生成物 | 3-Bromo-5-trifluoromethylphenyl 4-tolyl sulphide | HCID 19764849 | 63% |
反応手順
Using a similar procedure to that described in the 1st paragraph of Note a. above 4-toluenethiol was reacted with 1-bromo-3-fluoro-5-trifluoromethylbenzene to give 3-bromo-5-trifluoromethylphenyl 4-tolyl sulphide in 63% yield as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05208259 |
| 出典データセット | uspto-grants-1993_05 |
| ORD ID | ord-bdb4bed397164cd9a7fef44ca74741dc |
| 出典メモ | uspto-grants-1993_05 |