化工社化工社 化学情報印刷レポート · 研究参考用
tert-Butyl hydroperoxide → t-Amylperoxy 2,4-dimethylphenyl carbonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl hydroperoxide | HCID 6410 | — |
| 反応物 | Phenyl chloroformate | HCID 15891 | — |
| 反応物 | tert-Amyl hydroperoxide | HCID 76962 | — |
| 反応物 | 2,4-Dimethylphenyl chloroformate | HCID 15917593 | — |
| 生成物 | t-Amylperoxy 2,4-dimethylphenyl carbonate | HCID 54014625 | 65% |
反応手順
A reaction was carried out in the same manner as described in Example 1, except that t-amyl hydroperoxide and 2,4-dimethylphenyl chloroformate were used in place of t-butyl hydroperoxide and phenyl chloroformate used in Example 1, to obtain 35.7 g (yield: 65%) of a compound having a GLC purity of 92%, which was a colorless liquid at room temperature.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05210164 |
| 出典データセット | uspto-grants-1993_05 |
| ORD ID | ord-9738c85b397c400f9da90cbac3ec4e2f |
| 出典メモ | uspto-grants-1993_05 |