Hydrochloric Acid → HCID 22569398、化合物

HRID 24942ノート

反応式

HRID 24942 の反応式
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][N:12]([CH3:16])[CH2:13][CH2:14][NH2:15].Cl>C(O)C>[CH3:11][N:12]([CH3:16])[CH2:13][CH2:14][NH:15][C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 9590p-FluoronitrobenzeneHCID 66053N,N-Dimethylethylenediamine

生成物 1

HCID 22569398HCID 22569398、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

2.2 ml of (20 mmol) of 4-fluoronitrobenzene and 2.6 ml (24 mmol) of N,N-dimethylethylene-diamine are heated in 10 ml of ethanol at 120° C. in a microwave oven for 1.5 hours. Then 50 ml of 1 N hydrochloric acid are added. The reaction solution is washed with ethyl acetate. Then the aqueous phase is combined with 4 N sodium hydroxide solution until an alkaline reaction is obtained and extracted with ethyl acetate.

後処理

  1. washThe reaction solution is washed with ethyl acetate
  2. customThen the aqueous phase is combined with 4 N sodium hydroxide solution until an alkaline reaction
  3. customis obtained
  4. extractionextracted with ethyl acetate

出典と根拠

ORDレコード
ord-33970417aed54766919fad76ccaaf316
出典データセット
uspto-grants-2005_02
特許番号
US06855710B2

反応ノート

読み込み中…