Carbonic acid, bis[2-(dimethylamino)ethyl] ester → Bis(dimethylaminoethyl) ether
反応式
CN(CCO[C:7](=O)[O:8][CH2:9][CH2:10][N:11]([CH3:13])[CH3:12])C.[Mg].[Al]>>[CH3:13][N:11]([CH2:10][CH2:9][O:8][CH2:7][CH2:10][N:11]([CH3:13])[CH3:12])[CH3:12]参加物
4
実験手順
A process for preparing bis[2-(N,N-dimethylamino)ethyl]ether which comprises (i) contacting 2-(N,N-dimethylamino)ethanol with diethyl carbonate under conditions effective to produce bis[2-(N,N-dimethylamino)ethyl]carbonate, and (ii) contacting bis[2-(N,N-dimethylamino)ethyl]-carbonate with a magnesium:aluminum mixed metal oxide catalyst under conditions effective to produce bis[2-(N,N-dimethylamino)ethyl]ether.
出典と根拠
- ORDレコード
- ord-8e6c8389cda54e69bb49cc6488244b43
- 出典データセット
- uspto-grants-1993_05
- 特許番号
- US05214142
反応ノート
読み込み中…