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2-Chloro-5-(chloromethyl)pyridine → N-((2-Chlorothiazol-5-yl)methyl)ethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chloro-5-(chloromethyl)pyridine | HCID 155479 | — |
| 反応物 | 2-Chloro-5-chloromethylthiazole | HCID 2763179 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | N-((2-Chlorothiazol-5-yl)methyl)ethanamine | HCID 22450338 | — |
反応手順
The reaction procedure of Reference Example 17 was repeated except that crude 2-chloro-5-chloromethylthiazole was used in lieu of 6-chloro-3-pyridylmethyl chloride and that CH2Cl2 was used as the extractant. The procedure gave the title compound as a crude oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05214152 |
| 出典データセット | uspto-grants-1993_05 |
| ORD ID | ord-eef47cd986ac4f6abf30eb8c55e6c572 |
| 出典メモ | uspto-grants-1993_05 |