Hydrazine, (2-fluorophenyl)-, hydrochloride (1:1) → HCID 178515185、化合物
反応式
[C:1]1([N:7]2[C:19](=[O:20])[C:10]3=[CH:11][NH:12][C:13]4[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=4[C:9]3=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[F:22]C1C=CC=CC=1NN>>[F:22][C:6]1[CH:5]=[CH:4][CH:3]=[CH:2][C:1]=1[N:7]1[C:19](=[O:20])[C:10]2=[CH:11][NH:12][C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=3[C:9]2=[N:8]1参加物
3
実験手順
The title compound was prepared following the procedure described in Step 3 for the synthesis of 4a, using 2-fluorophenyl hydrazine hydrochloride instead of phenyl hydrazine hydrochloride. 1H NMR (DMSO-d6) δ (ppm): 7.13-7.46 (3H, m), 7.48-7.62 (2H, m), 7.67 (1H, dd, J=6.87, 1.37 Hz), 7.73 (1H, d, J=8.24 Hz), 8.11 (1H, dd, J=8.24, 1.09 Hz), 8.70 (1H, d, J=6.31 Hz). m/z 280.3 (MH+).
出典と根拠
- ORDレコード
- ord-5fe597adfea54e60a3e1fce297f4b574
- 出典データセット
- uspto-grants-2011_01
- 特許番号
- US07863266B2
反応ノート
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