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1-(Pyridin-2-yl)ethan-1-amine → N-((3-Methylpyridin-2-yl)methyl)-1-(pyridin-2-yl)ethanamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(Pyridin-2-yl)ethan-1-amine | HCID 541877 | — |
| 反応物 | 3-Methylpyridine-2-carboxaldehyde | HCID 1501874 | — |
| 反応物 | Sodium borohydride | HCID 4311764 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N-((3-Methylpyridin-2-yl)methyl)-1-(pyridin-2-yl)ethanamine | HCID 45098009 | 60% |
反応手順
Using General Procedure B, reaction of 1-Pyridin-2-yl-ethylamine and 3-methylpyridine-2-carbaldehyde in MeOH with NaBH4 gave (3-Methyl-pyridin-2-ylmethyl)-(1-pyridin-2-ylethyl)-amine as a pale yellow oil (0.21 g, 60%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07863293B2 |
| 出典データセット | uspto-grants-2011_01 |
| ORD ID | ord-3adc126131c84145a626891bb65446ca |
| 出典メモ | uspto-grants-2011_01 |