化工社化工社 化学情報印刷レポート · 研究参考用
1,2-Dichloroethane → Tropolone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2-Dichloroethane | HCID 11 | — |
| 反応物 | 5-Amino-2-hydroxy-2,4,6-cycloheptatrien-1-one | HCID 23450 | — |
| 反応物 | N-Hydroxysulfosuccinimide | HCID 133909 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 溶媒 | Carbonate Ion | HCID 19660 | — |
| 生成物 | Tropolone | HCID 10789 | — |
反応手順
To 100E6 carboxylated microspheres (previously activated with sulfo-N-hydroxysuccinimide and EDC) in 0.5 mL of carbonate buffer (pH 9) was added 2 mg of 5-aminotropolone dissolved in 25 μL of dimethyl sulfoxide. The suspension was agitated for 4 hours, and the excess reagent was washed away from the microspheres.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07867774B2 |
| 出典データセット | uspto-grants-2011_01 |
| ORD ID | ord-a3f5b91bacba4e389953cdb821e81d21 |
| 出典メモ | uspto-grants-2011_01 |