(+)-Lactose → HCID 178438163、化合物

HRID 251793

反応式

HRID 251793 の反応式
[CH3:1][CH2:2][C@@:3]12[C@:11]([O:14][C:15]([CH3:17])=[O:16])([C:12]#[CH:13])[CH2:10][CH2:9][C@H:8]1[C@@H:7]1[CH2:18][CH2:19][C:20]3[C@@H:27]([C@H:6]1[CH2:5][CH2:4]2)[CH2:26][CH2:25]/[C:22](=[N:23]\[OH:24])/[CH:21]=3.[OH:28][CH:29]1[O:48][C@H:47]([CH2:49][OH:50])[C@@H:34]([O:35][C@@H:36]2[O:44][C@H:43]([CH2:45][OH:46])[C@H:41]([OH:42])[C@H:39]([OH:40])[C@H:37]2[OH:38])[C@H:32]([OH:33])[C@H:30]1[OH:31]>>[CH3:1][CH2:2][C@@:3]12[C@:11]([O:14][C:15]([CH3:17])=[O:16])([C:12]#[CH:13])[CH2:10][CH2:9][C@H:8]1[C@@H:7]1[CH2:18][CH2:19][C:20]3[C@@H:27]([C@H:6]1[CH2:5][CH2:4]2)[CH2:26][CH2:25]/[C:22](=[N:23]\[OH:24])/[CH:21]=3.[OH:28][CH:29]1[O:48][C@H:47]([CH2:49][OH:50])[C@@H:34]([O:35][C@@H:36]2[O:44][C@H:43]([CH2:45][OH:46])[C@H:41]([OH:42])[C@H:39]([OH:40])[C@H:37]2[OH:38])[C@H:32]([OH:33])[C@H:30]1[OH:31]

参加物

3

反応物 2

HCID 440995(+)-Lactose3 回HCID 6540478Norgestimate

生成物 1

HCID 178438163HCID 178438163、化合物

実験手順

Norgestimate (2.2 mg) and lactose (2.6 mg) were mixed with a spatula in a vial for 1 minute. Additional amounts of lactose (4.6 mg) were added and then mixed with a spatula for another minute. This was repeated until all of the lactose was added (9.0 mg, 2.6 mg, total of 18.8 mg).

後処理

  1. additionmixed with a spatula for another minute
  2. additionwas added (9.0 mg, 2.6 mg, total of 18.8 mg)

出典と根拠

ORDレコード
ord-e49ba1dba07240a2b1a8dfc80d6088c9
出典データセット
uspto-grants-2011_01
特許番号
US07867990B2

関連ノート

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