関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetate | HCID 175 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Aluminum Acetate | HCID 8757 | — |
反応手順
Aqueous basic aluminum chloride solution of concentration of 5.0% by weight on the basis of Al2O3 was produced by diluting commercialized aqueous basic aluminum chloride solution (23.5% by weight on the basis of Al2O3, 8.15% by weight of chloride ion, 83.3% of basicity, and pH 4.0) with pure water. The aqueous solution was passed through an acetate-type anion exchange resin column at space velocity 5 to obtain an aqueous basic aluminum acetate solution. The obtained aqueous solution was dried at 90° C. and atmospheric pressure to adjust the water content to be 20% to obtain a basic aluminum acetate solid. The obtained solid had 0.79 in a full width at half maximum of the peak measured by the x-ray diffractiometry described in the above-mentioned evaluation method.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US07868126B2 |
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| 出典データセット | uspto-grants-2011_01 |
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| ORD ID | ord-ec8c49b5b9d944bc9efc1dbd783b8dd4 |
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| 出典メモ | uspto-grants-2011_01 |
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