関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Propiolic Acid | HCID 10110 | — |
| 反応物 | 1-Azidododecane | HCID 10998318 | — |
| 生成物 | 1-Dodecyl-1H-1,2,3-triazole-4-carboxylic acid | HCID 63467685 | — |
反応手順
A mixture of propiolic acid (46 μL, 0.7419 mmol) and 1-azido-dodecane (156.8 mg, 0.7419 mmol) was heated to 120° C. in a capped vial for 14 h, to yield the title triazole as white, crystalline solid (189.3 mg, 91% yield). The product was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07868135B2 |
|---|
| 出典データセット | uspto-grants-2011_01 |
|---|
| ORD ID | ord-eb3be02f342142e3bc24729ff2e33713 |
|---|
| 出典メモ | uspto-grants-2011_01 |
|---|
