化工社化工社 化学情報印刷レポート · 研究参考用
4-Nitroindazole → NoName_3327
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Nitroindazole | HCID 18057 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | NoName_3327 | HCID 413085 | 101.3% |
反応手順
A mixture of 4-nitro-1H-indazole (760 mg, 4.68 mmol), palladium on charcoal (10%, cat.) and ethanol (30 mL) was stirred under a balloon of hydrogen for 4 hours. The reaction mixture was then filtered through celite, and the solvent removed in vacuo to yield 1H-indazol-4-ylamine (68) (631 mg, 100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07872003B2 |
| 出典データセット | uspto-grants-2011_01 |
| ORD ID | ord-fa3777e0d9a04dadb1f178fb5c3866d4 |
| 出典メモ | uspto-grants-2011_01 |