1-Naphthylamine → Ethyl N-naphthalen-1-ylpropionimidate

反応式

[NH2:1][C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.[CH2:12]([O:14][C:15](OCC)(OCC)[CH2:16][CH3:17])[CH3:13]>>[C:2]1([N:1]=[C:15]([O:14][CH2:12][CH3:13])[CH2:16][CH3:17])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1

参加物

反応物 2

HCID 86401-Naphthylamine

HCID 66995Ethyl orthopropionate

生成物 1

HCID 66852489Ethyl N-naphthalen-1-ylpropionimidate

実験手順

The title compound was prepared from 1-aminonaphthalene and triethylorthopropionate according to the following procedure: DeWolfe, R. H. J. Org. Chem. 1962, 27, 490-493.

出典と根拠

ORDレコード: ord-1153dfed24d7403dab0940ff3c5aa2e7
出典データセット: uspto-grants-2011_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07875640B2

反応ノート

読み込み中…