化工社化工社 化学情報印刷レポート · 研究参考用
Benzyl Alcohol → Benzyl fluoroformate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyl Alcohol | HCID 244 | — |
| 反応物 | Sodium Fluoride | HCID 5235 | — |
| 反応物 | Acetonitrile | HCID 6342 | — |
| 反応物 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 生成物 | Benzyl fluoroformate | HCID 3023023 | — |
反応手順
The process is performed as in Example 1 with, in the first reactor, 168 g (4 mol) of sodium fluoride powder having the same characteristics as described in Example 1 and 320 ml of acetonitrile and, in the second reactor, 108 g (1 mol) of benzyl alcohol, 50.5 g (1.2 mol) of sodium fluoride of the same characteristics as above and 150 g of dimethoxyethane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858751B1 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-868776c4aa2e4da9aec0e9e64cce3e8d |
| 出典メモ | uspto-grants-2005_02 |