Sodium Trifluoroacetate → N-methoxymethyl-N-methylpyrrolidinium trifluoroacetate
反応式
[F:1][C:2]([F:7])([F:6])[C:3]([O-:5])=[O:4].[Na+].[Cl-].[CH3:10][O:11][CH2:12][N+:13]1([CH3:18])[CH2:17][CH2:16][CH2:15][CH2:14]1>CO>[F:1][C:2]([F:7])([F:6])[C:3]([O-:5])=[O:4].[CH3:10][O:11][CH2:12][N+:13]1([CH3:18])[CH2:17][CH2:16][CH2:15][CH2:14]1参加物
4
実験手順
In 100 g of methanol dissolved 14.94 g of sodium trifluoroacetate. To the solution was added 18.20 g of N-methoxymethyl-N-methylpyrrolidinium chloride and the mixture was stirred for 1 hour, concentrated in a vacuum and dried with use of a vacuum pump. The resulting product was dissolved in 500 ml of dichloromethane and the mixture was filtered with membrane filter, concentrated in a vacuum and dried in a vacuum to obtain 26.52 g of the desired product (colorless liquid). The product was checked for 1H-NMR, electrical conductivity and voltage resistance.