戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 25507作成日:2026年10月26日

Benzoic acid, 3-isothiocyanato- → 3-{3-[5-(5,6-Dichloro-1H-indol-2-yl)-2-methoxy-phenyl]-thioureido}-benzoic acid

https://huagongshe.com/reaction/25507

反応式

関与物質

役割名称HCID仕込み量
反応物Benzoic acid, 3-isothiocyanato-HCID 75046—
反応物5-(5,6-dichloro-1H-indol-2-yl)-2-methoxy-phenylamineHCID 9836191—
生成物3-{3-[5-(5,6-Dichloro-1H-indol-2-yl)-2-methoxy-phenyl]-thioureido}-benzoic acidHCID 10140976—

反応手順

3-{3-[5-(5,6-Dichloro-1H-indol-2-yl)-2-methoxy-phenyl]-thioureido}-benzoic acid was prepared from the product of Example 18, Step D, 5-(5,6-dichloro-1H-indol-2-yl)-2-methoxy-phenylamine (0.64 g, 1.72 mmol) and 3-carboxyphenyl isothiocyanate (0.359 g, 2.0 mmol) to give the product as a reddish-tan solid (0.104 g), mp 216-218° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06858739B2
出典データセットuspto-grants-2005_02
ORD IDord-fc2f96c8487d4e54b033454790b8d562
出典メモuspto-grants-2005_02