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2-Benzothiazolamine, 6-(methylsulfonyl)- → Adamantane-1-carboxylic acid (6-methanesulfonyl-benzothiazol-2-yl)-amide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Benzothiazolamine, 6-(methylsulfonyl)- | HCID 87152 | — |
| 反応物 | 1-Adamantanecarbonyl chloride | HCID 98915 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | Adamantane-1-carboxylic acid (6-methanesulfonyl-benzothiazol-2-yl)-amide | HCID 5000635 | — |
反応手順
Commercially available 6-methanesulfonyl-benzothiazol-2-ylamine, triethylamine, and adamantane-1-carbonyl chloride were processed as described for Example 17A to afford the title compound MS (ESI+) m/z 391 (M+H)+;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07875639B2 |
| 出典データセット | uspto-grants-2011_01 |
| ORD ID | ord-1c435597e1364840be9cbd59bd11f7e2 |
| 出典メモ | uspto-grants-2011_01 |