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Thiophosgene → [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thiophosgene | HCID 10040 | — |
| 反応物 | 5-(1H-indol-2-yl)-2-methoxy-phenylamine | HCID 9900204 | — |
| 生成物 | [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate | HCID 22568433 | — |
反応手順
The product from Example 1, 5-(1H-indol-2-yl)-2-methoxy-phenylamine, (4.76 g, 20 mmol) was reacted with thiophosgene (1.9 mL, 25 mmol) according to the procedure for Example 23, Step A, to give [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate (4.55 g), as a black solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858739B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-0fec09881fb740ff8ab79f4f7634b1cd |
| 出典メモ | uspto-grants-2005_02 |