化工社化工社 化学情報印刷レポート · 研究参考用
1,6-Dibromohexane → HCID 178486059、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,6-Dibromohexane | HCID 12368 | — |
| 反応物 | HCID 178486055 | HCID 178486055 | — |
| 生成物 | HCID 178486059 | HCID 178486059 | — |
反応手順
In analogy to examples 1.4 and 1.5, trans-(4-Hydroxy-cyclohexyl)-methyl-carbamic acid tert-butyl ester was reacted with 1,6-dibromohexane to yield trans-[4-(6-Bromo-hexyloxy)-cyclohexyl]-methyl-carbamic acid tert-butyl ester which was reacted with N-allylmethylamine to yield trans-(4-[6-(Allyl-methyl-amino)-hexyloxy]-cyclohexyl)-methyl-carbamic acid tert-butyl ester as light brown oil, MS: 382 (M).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858651B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-6bcf74ab6ce04373a5f3ec962cac2747 |
| 出典メモ | uspto-grants-2005_02 |