化工社化工社 化学情報印刷レポート · 研究参考用
1,7-Dibromoheptane → HCID 178486060、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,7-Dibromoheptane | HCID 78309 | — |
| 反応物 | HCID 178486055 | HCID 178486055 | — |
| 生成物 | HCID 178486060 | HCID 178486060 | — |
反応手順
In analogy to examples 1.4 and 1.5, trans-(4-Hydroxy-cyclohexyl)-methyl-carbamic acid tert-butyl ester was reacted with 1,7-dibromoheptane to yield trans-[4-(7-Bromo-heptyloxy)-cyclohexyl]-methyl-carbamic acid tert-butyl ester which was reacted with N-allylmethylamine to yield trans-(4-[7-(Allyl-methyl-amino)-heptyloxy]-cyclohexyl)-methyl-carbamic acid tert-butyl ester as colorless oil, MS: 397 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06858651B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-b5bc525e09a04804842b7d1f8dbc3a4a |
| 出典メモ | uspto-grants-2005_02 |