1-(2-Nitropropoxy)-2,2,5,5-tetramethylcyclopentane → HCID 13878920、化合物
反応式
[N+:1]([CH:4]([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14])([O-])=O>CO.[Ni]>[NH2:1][CH:4]([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14]参加物
4
実験手順
1-(2-Nitropropoxy)-2,2,5,5-tetramethylcyclopentane is dissolved in methanol and hydrogenated at 50 psi with Raney nickel T-1 as a catalyst. The reaction mixture is filtered through Celite and evaporated to yield 1-(2-aminopropoxy)-2,2,5,5-tetramethylcyclopentane.
後処理
- filtrationThe reaction mixture is filtered through Celite
- customevaporated
出典と根拠
- ORDレコード
- ord-c237420f04314ad38502463442e85d65
- 出典データセット
- uspto-grants-1987_10
- 特許番号
- US04698231
反応ノート
読み込み中…