1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane → 1-(2-Amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane

HRID 255461

反応式

[N+:1]([C:4]([CH3:17])([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14])([O-])=O>CO.[Ni]>[NH2:1][C:4]([CH3:17])([CH3:16])[CH2:5][O:6][CH:7]1[C:11]([CH3:13])([CH3:12])[CH2:10][CH2:9][C:8]1([CH3:15])[CH3:14]

参加物

実験手順

1-(2-Nitro-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane is dissolved in methanol and hydrogenated at 50 psi with Raney nickel T-1 as a catalyst. The reaction mixture is filtered through Celite and evaporated to yield 1-(2-amino-2-methylpropoxy)-2,2,5,5-tetramethylcyclopentane.

後処理

filtrationThe reaction mixture is filtered through Celite
customevaporated

出典と根拠

ORDレコード: ord-072cd696dd184a92a527b40d5e77fb5d
出典データセット: uspto-grants-1987_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04698231

反応式

参加物

反応物 1

生成物 1

試薬・触媒・溶媒 2

実験手順

後処理

出典と根拠

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